{"created":"2025-02-06T04:20:53.731485+00:00","id":2013220,"links":{},"metadata":{"_buckets":{"deposit":"1f98ecfb-ba9d-45de-9be3-f2879c66f60d"},"_deposit":{"created_by":10,"id":"2013220","owner":"92","owners":[10],"pid":{"revision_id":0,"type":"depid","value":"2013220"},"status":"published"},"_oai":{"id":"oai:fra.repo.nii.ac.jp:02013220","sets":["15"]},"author_link":["2597","1054","453","524","718"],"control_number":"2013220","item_10001_biblio_info_7":{"attribute_name":"書誌情報","attribute_value_mlt":[{"bibliographicIssueDates":{"bibliographicIssueDate":"2024-10-25","bibliographicIssueDateType":"Issued"},"bibliographicIssueNumber":"5","bibliographicNumberOfPages":"7","bibliographicPageEnd":"135","bibliographicPageStart":"129","bibliographicVolumeNumber":"65","bibliographic_titles":[{"bibliographic_title":"食品衛生学雑誌","bibliographic_titleLang":"ja"}]}]},"item_10001_description_5":{"attribute_name":"抄録","attribute_value_mlt":[{"subitem_description":"ホタテガイ中の麻痺性貝毒11成分の妥当性評価試験を実施し，Codexの定める検査法の性能規準を満たしているかを確認した．加えて，近年国内外の二枚貝中よりフグ毒テトロドトキシン（TTX）の含有が報告されていることから，本試験の対象成分とした．Turnerらの方法に従って試験を実施し，溶媒検量線およびマトリックス検量線（ホタテガイ）で定量を行った．妥当性評価の結果は，麻痺性貝毒11成分で目標値（真度，併行精度，室内精度）を満たしたが，TTXを溶媒検量線で定量した場合に低回収率となった．一方で，TTXをマトリックス検量線（ホタテガイ）で定量した場合に，回収率が改善した．以上の結果から，本法はLC-MS/MSを用いた麻痺性貝毒およびTTXの分析について有用な分析法であると考えられるが，適切な検量線の選択が必要であることが示唆された．","subitem_description_language":"ja","subitem_description_type":"Abstract"}]},"item_10001_publisher_8":{"attribute_name":"出版者","attribute_value_mlt":[{"subitem_publisher":"日本食品衛生学会","subitem_publisher_language":"ja"}]},"item_10001_relation_14":{"attribute_name":"DOI","attribute_value_mlt":[{"subitem_relation_type":"isIdenticalTo","subitem_relation_type_id":{"subitem_relation_type_id_text":"10.3358/shokueishi.65.129","subitem_relation_type_select":"DOI"}}]},"item_10001_relation_16":{"attribute_name":"情報源","attribute_value_mlt":[{"subitem_relation_name":[{"subitem_relation_name_language":"ja","subitem_relation_name_text":"水産技術研究所 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